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Synthesis and characterization of (cyclopentadienyl)titanium(IV) complexes of 1,3-dihydro-1,3-dioxo-alpha-(substituted)-2H-isoindole 2-acetates

Complexes having the general formulae (C5H5)2TiCl(L), C5H5)TiCl(L)2 and (C5H5)2Ti(L)2, have been synthesized by the reactions of N-protected amino acids (LH), (where R = -H, -CH(CH3)2, -CH2C6H5, -CH2CH2SCH3 and -CHR- = -CH2CH2-) with titanocene dichloride in the presence of triethylamine in refluxing tetrahydrofuran.These derivatives have been characterized by elemental analyses, molecular weight measurements, and IR, 1H and 13C NMR spectral studies.

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Reference£º
Metal catalyst and ligand design,
Ligand Template Strategies for Catalyst Encapsulation – NCBI