348-67-4, H-D-Met-OH is a catalyst-ligand compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
Step (1): To a 2 L four-necked flask was added 153.10 g of D-methionine, 420 g of water, 200 mL of methanol and 158.21 g of diethyl sulfate, and the mixture was stirred at room temperature, and 45 g of concentrated sulfuric acid After the end of heating to 30 ~ 40 , 10h, the recovery of methanol under reduced pressure.After the reaction with anhydrous sodium carbonate solid to adjust the pH to 8 ~ 9, continue 40 reaction 10h.After the reaction is over,The solvent was distilled off under reduced pressure.
348-67-4, 348-67-4 H-D-Met-OH 84815, acatalyst-ligand compound, is more and more widely used in various fields.
Reference£º
Patent; Anhui Zhishan New Materials Co., Ltd.; Wei Kaiju; Ren Mingxiu; Cui Yang; Chen Zhongming; Xie Yineng; (9 pag.)CN106928110; (2017); A;,
Metal catalyst and ligand design
Ligand Template Strategies for Catalyst Encapsulation – NCBI