Analyzing the synthesis route of 6813-38-3

As the paragraph descriping shows that 6813-38-3 is playing an increasingly important role.

6813-38-3, [2,2′-Bipyridine]-4,4′-dicarboxylic acid is a catalyst-ligand compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated

6813-38-3, Take the product I obtained 2g and 10mL 98% H2SO4, 100mL CH3OH into the flask with a stirrer, reflux at 105 C overnight, the end of the reaction to a large amount of water appears white flocculent precipitate, slowly adding NaOH solution adjusted to pH 9.0 , With CH2C12 extract to retain the organic phase, anhydrous Na2S04 dry, evaporated to dry the solvent to obtain white crystals, the yield of 88%.

As the paragraph descriping shows that 6813-38-3 is playing an increasingly important role.

Reference£º
Patent; Nanjing University of Posts and Telecommunications; Zhao, Qiang; Huang, Wei; Huang, Tianci; Liu, Shujuan; Xu, Wenjuan; Zhu, Yana; (10 pag.)CN106188151; (2016); A;,
Metal catalyst and ligand design
Ligand Template Strategies for Catalyst Encapsulation – NCBI