7328-91-8, 2,2-Dimethylpropane-1,3-diamine is a catalyst-ligand compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
2,2-dimethylpropane-1,3-diamine (5.0?g, Aldrich) was added to a solution of HCOOH (10 equiv) and HCHO (37% aqueous solution, 10?equiv), and was heated at reflux overnight, whereupon the solution was made basic by addition of NaOH (2?M, aqueous) and extracted into diethyl ether (4?*?25?mL). The ether solution was dried over K2CO3, and the solvent removed by rotary evaporation. The resulting oil was distilled in vacuo from CaH2 to afford the product as a colorless oil (75%). 1H NMR (CDCl3, 400?MHz): delta 0.9 (m, 6H); 2.0 (m, 4H); 2.2 (m, 12H). GC-MS: [60?C (1?min) to 180?C (2?min) at 30?C¡¤min-1]; tr?=?5.2?min (158, M+)., 7328-91-8
As the paragraph descriping shows that 7328-91-8 is playing an increasingly important role.
Reference£º
Article; Large, Tao A.G.; Mahadevan, Viswanath; Keown, William; Stack, T. Daniel P.; Inorganica Chimica Acta; vol. 486; (2019); p. 782 – 792;,
Metal catalyst and ligand design
Ligand Template Strategies for Catalyst Encapsulation – NCBI