148332-36-9, [2,2′:6′,2”-Terpyridine]-4′-carboxylic acid is a catalyst-ligand compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
1.0 mmol of CuSO4 and 0.5 mmol of 2,2 ‘:6′,2″-terpyridine-4’-carboxylic acid were mixed, and placed in a stainless steel-lined stainless steel reactor. 20 mL of deionized water and 10 mL of absolute ethanol were added, mixed evenly, sealed, and hydrothermal reaction was carried out at 120-180 ¡ã C for 3 ~ 5 days under high temperature and high pressure environment to increase the reaction. The oxidation-reduction potential of the material changes significantly to improve the reaction rate. After completion of the hydrothermal reaction, the stainless steel reactor was cooled to room temperature by 5 ¡ã C per hour to obtain a blue block of 2,2 ‘: 6’, 2 ‘tripyridine-4’-carboxylic acid copper sulfate crystals. The resulting crystals were ground to 100 mesh sieve, to obtain terpyridine-4 ‘-carboxylic acid copper hydrogensulfate monoclinic blue powder having purity of not less than 99percent., 148332-36-9
The synthetic route of 148332-36-9 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; Ningbo University; Lin, Danfeng; Xu, Wei; Zhang, Beibei; Qi, Jinli; Lin, Jianli; Zhu, Honglin; Zheng, Yueqing; (7 pag.)CN103450228; (2016); B;,
Metal catalyst and ligand design
Ligand Template Strategies for Catalyst Encapsulation – NCBI