Category: 13093-04-4

Some tips on 13093-04-4

13093-04-4, As the paragraph descriping shows that 13093-04-4 is playing an increasingly important role.

13093-04-4, N1,N6-Dimethylhexane-1,6-diamine is a catalyst-ligand compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated

To a four-neck 2000 mL RBF fitted with overhead stirrer, addition funnel, reflux condenser, and thermocouple, under N2, was added maleic anhydride (75g, 0.734 mol, 2.5 eq.) and dry acetonitrile (400 mL), followed by the dropwise addition of N,N’-dimethyl-1,6-hexanediamine (51.9 mL, 0.294 mol, 1 eq.), maintaining <30C. The reaction turned an orange color as the addition progressed. The reaction was heated to 450C for 2 hours, then stirred overnight at room temperature. By morning, a tan solid had precipitated. It was filtered, then dried to constant weight, giving 87.6 g (87%) of the desired product as an off-white solid. 13093-04-4, As the paragraph descriping shows that 13093-04-4 is playing an increasingly important role.

Reference£º
Patent; E. I. DU PONT DE NEMOURS AND COMPANY; WO2006/66031; (2006); A1;,
Metal catalyst and ligand design
Ligand Template Strategies for Catalyst Encapsulation – NCBI

Simple exploration of 13093-04-4

13093-04-4, As the paragraph descriping shows that 13093-04-4 is playing an increasingly important role.

With the rapid development and complex challenges of chemical substances, new drug synthesis pathways are usually the most effective.13093-04-4,N1,N6-Dimethylhexane-1,6-diamine,as a common compound, the synthetic route is as follows.

EXAMPLE III N,N’-Dimethyl-N,N’-hexamethylene-bis[3-(N,N-dibenzyl aminoxy)propionamide] A solution of 6.4 g of 3-(N,N-dibenzylaminoxy) propanoic acid in 25 ml of methylene chloride is admixed with 1.8 ml of oxalyl chloride at 0-5 C. After 2 hours, a solution of 8.61 g N,N’-dimethyl hexamethylenediamine in 25 ml of methylene chloride is added at 0 C. and the reaction mixture is stirred at room temperature for 12 hours. The insoluble salt residue is removed by filtration and methylene chloride is removed under reduced pressure. Purification by liquid chromatography affords the title compound as a thick oil.

13093-04-4, As the paragraph descriping shows that 13093-04-4 is playing an increasingly important role.

Reference£º
Patent; Ciba-Geigy Corporation; US4760179; (1988); A;,
Metal catalyst and ligand design
Ligand Template Strategies for Catalyst Encapsulation – NCBI