With the rapid development and complex challenges of chemical substances, new drug synthesis pathways are usually the most effective.17217-57-1,4,4′-Dimethoxy-2,2′-bipyridine,as a common compound, the synthetic route is as follows.
General procedure: 4,4?-Dmo-2,2?-bpy (0.22 g, 1 mmol) was placed in oneof the arms of a branched tube [32], and zinc(II) acetatedihydrate (0.11 g, 0.5 mmol) and potassium thiocyanate(0.10 g, 1 mmol) were placed in the other arm. Ethanoland water in a ratio of 3:2 were carefully added to fill botharms. The tube was then sealed and the ligand-containingarm was immersed in a bath at 60¡ãC, whereas the otherwas maintained at ambient temperature. After 1 day, crystalsthat were deposited in the cooler arm were filtered off,washed with mother liquid, and dried in air, yield: 0.18 g,59percent.
As the paragraph descriping shows that 17217-57-1 is playing an increasingly important role.
Reference£º
Article; Marandi, Farzin; Moeini, Keyvan; Rudbari, Hadi Amiri; Zeitschrift fur Naturforschung, B: Chemical Sciences; vol. 71; 9; (2016); p. 959 – 965;,
Metal catalyst and ligand design
Ligand Template Strategies for Catalyst Encapsulation – NCBI