Category: 2390-68-3

With the rapid development and complex challenges of chemical substances, new drug synthesis pathways are usually the most effective.2390-68-3,N-Decyl-N,N-dimethyldecan-1-aminium bromide,as a common compound, the synthetic route is as follows.

Example 3. Preparation of Didecyldimethylammonium-Omadine Compounds[0069] Didecyldimethylamonium bromide (81.4 g, 75%> gel in water, 0.17 mol) was added to sodium omadine (56 ml, 28.2g, 0.2 mol) solution, mixed well and stirred for 2 hrs. Collect the desired product (top brown oil) and wash it with braine (saturated NaCl solution), dry it. Weight 102.2g (133%) yield containing water, structure is not fully assigned yet with NMR).

As the paragraph descriping shows that 2390-68-3 is playing an increasingly important role.

Reference£º
Patent; LIU, Huiwen; ZHANG, Boke; WO2012/12049; (2012); A2;,
Metal catalyst and ligand design
Ligand Template Strategies for Catalyst Encapsulation – NCBI

With the rapid development and complex challenges of chemical substances, new drug synthesis pathways are usually the most effective.2390-68-3,N-Decyl-N,N-dimethyldecan-1-aminium bromide,as a common compound, the synthetic route is as follows.

Decyldimethylammonium bromide (0.001 mol) was dissolved in 60 mL of distilled water by gentle heating and stirring. Sodium dihexylsulfosuccinate (Colawet MA-80 from Colonial Chemicals, South Pittsburg, Tenn.; 0.001 mol) was dissolved in 60 mL of distilled water by gentle heating and stirring. The two solutions were combined and the reaction mixture was heated and stirred for 30 minutes. The reaction mixture cooled to room temperature and then 60 mL of chloroform was added. The reaction mixture was stirred for an additional 30 minutes. The two phases were separated and the chloroform phase was washed several times with cool distilled water to remove any inorganic salt. The presence of chloride anions was monitored by silver nitrate test. A rotary evaporator removed the chloroform and a yellowish viscous liquid was obtained in 96.93% yield. 1H and 13C NMR (DMSO) were obtained. Melting point (hot plate apparatus)=liquid at room temperature. Thermal data determined by thermalgravimetric analysis (TGA): Tonset5%=218 C. and Tonset=226 C.

2390-68-3 N-Decyl-N,N-dimethyldecan-1-aminium bromide 16957, acatalyst-ligand compound, is more and more widely used in various.

Reference£º
Patent; Rogers, Robin D.; Daly, Daniel T.; Swatloski, Richard P.; Hough, Whitney L.; Davis, James Hilliard; Smiglak, Marcin; Pernak, Juliusz; Spear, Scott K.; US2007/93462; (2007); A1;,
Metal catalyst and ligand design
Ligand Template Strategies for Catalyst Encapsulation – NCBI