With the rapid development and complex challenges of chemical substances, new drug synthesis pathways are usually the most effective.14162-94-8,4-Chloro-2,2′-bipyridine,as a common compound, the synthetic route is as follows.
General procedure: For compound 1, a 1.0 mL aqueous solution of Ni(ClO4)2¡¤6H2O (0.005mmol) was placed at the bottom of a tube, a mixture of methanol and water (1:2, v/v, 3 mL)was gently layered on the top of the solution, and then a 1.0 mL methanol solutionof Bu4N[Fe(Tp*)(CN)3] (0.005 mmol) and 4-chlorine-2,2?-dibipyridine (0.01 mmol)was carefully added as the top layer. After few weeks, red block crystals were obtained,washed with water and air dried.
14162-94-8, The synthetic route of 14162-94-8 has been constantly updated, and we look forward to future research findings.
Reference£º
Article; Jiao, Yu-Shu; Jiao, Cheng-Qi; Meng, Yin-Shan; Liu, Xue-Ru; Zhao, Liang; Liu, Tao; Inorganic Chemistry Communications; vol. 93; (2018); p. 87 – 91;,
Metal catalyst and ligand design
Ligand Template Strategies for Catalyst Encapsulation – NCBI