Downstream synthetic route of 168646-54-6

The synthetic route of 168646-54-6 has been constantly updated, and we look forward to future research findings.

168646-54-6, 5,6-Diamino-1,10-phenanthroline is a catalyst-ligand compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated

168646-54-6, 0.33 g of 4,4′-dinitrobenzil (1.0 mmol) and 0.21 g of 5,6-diamine-1,10-phenanthroline (1.0 mmol) were put into a 100 mL single-necked flask, 30 mL of glacial acetic acid was added, Stirring, reaction under nitrogen 2h. After the reaction was completed, the solvent was removed by rotary evaporation and spin-dried. An appropriate amount of dichloromethane was added and the mixture was stirred for 10 min. Filtration, rotary evaporation of the solvent. The resulting solid was recrystallized from absolute ethanol, suction filtered and dried in vacuo to give 0.352 g of pale yellow crystals, The yield is 78.6percent. The reaction is:

The synthetic route of 168646-54-6 has been constantly updated, and we look forward to future research findings.

Reference£º
Patent; Jiangnan University; Zheng Changge; Xie Chen; Li Mingyue; (8 pag.)CN105884833; (2016); A;,
Metal catalyst and ligand design
Ligand Template Strategies for Catalyst Encapsulation – NCBI