With the rapid development and complex challenges of chemical substances, new drug synthesis pathways are usually the most effective.348-67-4,H-D-Met-OH,as a common compound, the synthetic route is as follows.
Methionine (0.3 mmol,)And NaOH (0.3 mmol) were dissolved in 30 ml of a mixed solvent (VC2H5OH: VH2O = 5: 1)Stirring for 5 hours,So that it is fully dissolved; then add CuCl2 (0.3mmol),Stirring for 24 hours;Then, 3,4,7,8-tetramethyl-1,10-phenanthroline (0.3 mmol) was added,Stirring for 48 hours;Filter, take its clear liquid into 20ml of small test tube, the ether added to the filtrate above the filtrate and ether volume ratio is about 1: 2.5, standing, about a week after the blue crystal., 348-67-4
The synthetic route of 348-67-4 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; Capital Normal University; Lu, Xiaoming; Zhang, Bo; Zhang, Weichuan; Cheng, Yifeng; Sun, Xiaojing; (60 pag.)CN105440059; (2016); A;,
Metal catalyst and ligand design
Ligand Template Strategies for Catalyst Encapsulation – NCBI