787-70-2, [1,1′-Biphenyl]-4,4′-dicarboxylic acid is a catalyst-ligand compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated,787-70-2
A mixture of H2BPDC (0.097g, 0.4mmol), Melamine (0.050g, 0.4mmol), DMF (4mL), ethanol (4mL) and H2O (4mL) was sealed into a 20mL Teflon-lined stainless-steel reactor and heated at 105C for 3days under autogenous pressure, and then followed by slowly cooling to room temperature at a rate of 1.7C¡¤h-1. The obtained flavescens cuboid-like crystals of 1 were collected (yield: 80 % based on Melamine) after washing with ethanol and drying in air. Elemental analysis: calcd. (%) for C20H30N12O8: C: 42.40, H: 5.34, N: 29.67, O: 22.59; found: C: 42.11, H: 5.81, N: 29.32, O: 22.76. FT-IR (KBr, 4000-500cm-1)=3380(w), 2667(w), 1890(m), 1686(vs), 1632(s), 1509(vs), 1390(m), 1205(m), 1009(w), 1004(m), 850(s), 760(s), 700(s) cm-1.
The synthetic route of 787-70-2 has been constantly updated, and we look forward to future research findings.
Reference£º
Article; Liu, Ruichao; Liu, Jie; Yan, Xiangzhen; Yuan, Chunxue; Polyhedron; vol. 157; (2019); p. 1 – 5;,
Metal catalyst and ligand design
Ligand Template Strategies for Catalyst Encapsulation – NCBI