Extended knowledge of 3393-45-1

Here is a brief introduction to this compound(3393-45-1)Application In Synthesis of 5,6-Dihydro-2H-pyran-2-one, if you want to know about other compounds related to this compound(3393-45-1), you can read my other articles.

In general, if the atoms that make up the ring contain heteroatoms, such rings become heterocycles, and organic compounds containing heterocycles are called heterocyclic compounds. An article called Novel multi-dentate phosphines for Pd-catalyzed alkoxycarbonylation of alkynes promoted by H2O additive, published in 2019-03-31, which mentions a compound: 3393-45-1, Name is 5,6-Dihydro-2H-pyran-2-one, Molecular C5H6O2, Application In Synthesis of 5,6-Dihydro-2H-pyran-2-one.

A series of novel multi (bi-/tri-/tetra-)-dentate phosphines with good robustness against water and oxygen were synthesized and fully characterized. It was found that the developed ionic tri-dentate phosphine enabled Pd-catalyzed alkoxycarbonylation of alkynes with CO and alcs. which gave α,β-unsaturated esters RCH=CHCO2R1 [R = n-Bu, Ph, Bn, etc.; R1 = Me, Et, i-Pr, C6H11] and I using H2O as an additive instead of acid. As for ionic tri-dentate phosphine, its unique steric configuration with two types of potential P-P chelation modes (P···P distance of 4.31 Å and 4.36 Å resp.) to Pd-center rendered the corresponding Pd-catalyst high activity and good stability for alkoxycarbonylation of alkynes. The in situ FT-IR anal. also verified that the formation and stability of Pd-H active species were greatly facilitated with the presence of ionic tri-dentate phosphine as well as H2O additive. In addition, as an ionic phosphine, ionic tri-dentate phosphine based PdCl2(MeCN)2 system immobilized in RTIL of [Bmim]NTf2 could be recycled for 7 runs without obvious activity loss or metal leaching.

Here is a brief introduction to this compound(3393-45-1)Application In Synthesis of 5,6-Dihydro-2H-pyran-2-one, if you want to know about other compounds related to this compound(3393-45-1), you can read my other articles.

Reference:
Metal catalyst and ligand design,
Ligand Template Strategies for Catalyst Encapsulation – NCBI