1435-55-8, Hydroquinidine is a catalyst-ligand compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
From dihydroquinidine To a 0 C. solution of 1.22 g dihydroquinidine (0.0037 mol) in 30 mL of CH2 Cl2 was added 0.78 mL of Et3 N (0.0056 mol; 1.5 eq), followed by 0.71 mL of p-chlorobenzoyl chloride (0.005 mol; 1.2 eq) in 1 mL CH2 Cl2. After stirring 30 minutes at 0 C. and 1 hour at room temperature, the reaction was quenched by the addition of 10% Na2 CO3 (20 mL). After separation, the aqueous layer was extracted with three 10 mL portions of CH2 Cl2. The combined organic layers were dried over Na2 SO4 and the solvent removed under vacuum. The crude product was purified as described above. Dihydroquinidine p-chlorobenzoate (1) was obtained in 91% yield (1.5g) as a white foam., 1435-55-8
The synthetic route of 1435-55-8 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; Massachusetts Institute of Technology; US4871855; (1989); A;,
Metal catalyst and ligand design
Ligand Template Strategies for Catalyst Encapsulation – NCBI