23616-79-7, N-Benzyl-N,N-dibutylbutan-1-aminium chloride is a catalyst-ligand compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
EXAMPLE 6 P-NITROBENZYL (5R,6R)-6-(2′,2′-DIMETHYL-3′-NITROSO-5′-OXO-4′-PHENYL-IMIDAZOLIDIN-1′-YL)-3,3-DIMETHYL-7-OXO-4-THIA-1-AZABICYCLO[3,2,0]HEPTANE-2-CARBOXYLATE (X) A mixture of 4.2 g (10 mmol) of (5R,6R,4’R)-6-(2′,2′-dimethyl-3′-nitroso-5′-oxo-4′-phenyl-imidazolidin-1′-yl)-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo[3,2,0]heptane-2-carboxylic acid, 0.9 g (11 mmol) of sodium bicarbonate, 3.4 g (11 mmol) of benzyltributylammonium chloride, 2.16 g (10 mmol) of p-nitrobenzyl bromide and 42 ml of acetonitrile are stirred at room temperature for 1 hour. Then 50 ml of water are added and extraction is carried out with ethyl acetate. The extracts are washed successively with water and a saturated sodium chloride solution. Drying over anhydrous magnesium sulphate and subsequent evaporation are carried out, thereby obtaining the title product in the form of a solid.
The synthetic route of 23616-79-7 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; Antibioticos, S.A.; US5229509; (1993); A;,
Metal catalyst and ligand design
Ligand Template Strategies for Catalyst Encapsulation – NCBI