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Copper-Catalyzed Oxidative Cleavage of the C-C Bonds of beta-Alkoxy Alcohols and beta-1 Compounds
Copper-catalyzed aerobic oxidation conditions were employed to promote the C-C bond cleavage of beta-alkoxy alcohols and beta-1 compounds (lignin model compounds). Besides these compounds, various 1,2 and 1,3-diols were successfully converted to aldehydes. We propose the Cu(I)-catalyzed mechanism explaining the C-C cleavage of these 1,2 and 1,3-dihydroxy compounds and beta-alkory alcohols based on XPS data. Although our reaction conditions do not include large excess of bases and elaborated ligand-modified catalysts, copper salts with/without Me-TBD show good catalytic activities for C-C bond cleavage of various lignin model compounds.
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Reference:
Metal catalyst and ligand design,
,Ligand Template Strategies for Catalyst Encapsulation – NCBI