The preparation of ester heterocycles mostly uses heteroatoms as nucleophilic sites, which are achieved by intramolecular substitution or addition reactions. Compound: DL-Histidine monohydrochloride monohydrate( cas:123333-71-1 ) is researched.HPLC of Formula: 123333-71-1.Amoureux, Jean-Paul; Hu, Bingwen; Trebosc, Julien published the article 《Enhanced resolution in proton solid-state NMR with very-fast MAS experiments》 about this compound( cas:123333-71-1 ) in Journal of Magnetic Resonance. Keywords: magic angle spinning proton solid state NMR. Let’s learn more about this compound (cas:123333-71-1).
We present a new smooth amplitude-modulated (SAM) method that allows to observe highly resolved 1H spectra in solid-state NMR. The method, which works mainly at fast or ultra-fast MAS speed (ν R > 25 kHz) is complementary to previous methods, such as DUMBO, FSLG/PMLG or symmetry-based sequences. The method is very robust and efficient and does not present line-shape distortions or fake peaks. The main limitation of the method is that it requires a modern console with fast electronics that must be able to define the cosine line-shape in a smooth way, without any transient. However, this limitation mainly occurs at ultra-fast MAS where the rotation period is very short.
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Reference:
Metal catalyst and ligand design,
Ligand Template Strategies for Catalyst Encapsulation – NCBI