33454-82-9, Lithium trifluoromethanesulfonate is a catalyst-ligand compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
1.55 parts by mass of 4-methoxythioanisole, 1.95parts by mass of silver borofluoride, 1.77 parts by mass of 1 -chloromethyl naphthalene, and 10.0 parts by mass of acetone were uniformly mixed and reacted at 25 C. for 24 hours. Afier removal of silver chloride, the reaction solution was transferred to a rotary evaporator, and the solvent was distilled off. The obtained residue was reprecipitated with 10.0 parts by mass of acetone and 10.0 parts by mass of hexane. 3.44 parts by mass of the obtained precipitate, 1.56 parts by mass of lithium trifluoromethanesulfonate, and 10.0 parts by mass of acetone were uniformly mixed and reacted at 25C. for 24 hours. 10.0 parts by mass of distilled water were added to the reaction solution to wash the product. The solvent was distilled off under reduced pressure from the organic layer to obtain 3.87 parts by mass of compound 23. The ratio of the mass of the compound B to the total mass of the compound B and the compound A was 0.965. The yield with respect to 4-methoxythioanisole was 87%. The mass of the compound B was 3.73 g, and the mass of the compoundA was0.14g., 33454-82-9
The synthetic route of 33454-82-9 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; ASAHI KASEI E-MATERIALS CORPORATION; SHIMURA, Tadashi; KAMIMURA, Naoya; OTANI, Akira; SHIMADA, Hitoshi; (69 pag.)US2016/229801; (2016); A1;,
Metal catalyst and ligand design
Ligand Template Strategies for Catalyst Encapsulation – NCBI