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The synthesis and full characterization of new half-sandwich ruthenium(ii) complexes containing kappa3(N,N,N)-hydridotris(pyrazolyl)borate (kappa3(N,N,N)-Tp) and the water-soluble phosphanes 1,3,5-triaza-7-phosphatricyclo[3.3.1.13,7]decane (PTA) and 1-methyl-3,5-diaza-1-azonia-7-phosphatricyclo[3.3.1.13,7]decane (1-CH3-PTA) has been explored. Single crystal X-ray diffraction analysis for complex [RuCl{kappa3(N,N,N)-Tp}(PMe 2Ph)(1-CH3-PTA)][CF3SO3] ·2NCMe is also reported. DNA binding properties of the ruthenium complexes have been evaluated by mobility shift assay and MALDI-TOF mass spectrometry. The in vitro antitumor activity of these compounds was assessed by examining their ability to inhibit cell proliferation in a number of human cancer cell lines (NCI-H460, SF-268, MCF-7) and non-tumor human umbilical vein endothelial cells (HUVEC). Some of these new compounds show promising cytotoxic activity with IC50 values in the low micromolar range, and display differential effects on cancer and normal cell growth. The Royal Society of Chemistry 2010.
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Reference：
Metal catalyst and ligand design,
Ligand Template Strategies for Catalyst Encapsulation – NCBI