10108-87-9, N,N,N-Trimethyldecan-1-aminium chloride is a catalyst-ligand compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
General procedure: In the next step, alkyltrimethylammonium chlorides3a-c as prepared above (0.07 mol) were dissolved in ethanol(20 mL) and weighed precisely. The exact amount ofchloride ions was determined by AgNO3 titration of smallsamples and the required equimolar amounts of carboxylicacids 4a-c were weighted and added. 95% of KOH, requiredfor neutralization, was weighed as solid pellets. Afterall of the added solid KOH dissolved and KCl precipitated(1 hour), the remaining KOH was titrated as anapproximate 0.25 M solution of KOH in ethanol until potentialof glass electrode dropped below -250 mV whichwas previously determined as the potential of the inflectionpoint. Solutions were filtered to separate the filtrate containingthe products from the precipitated KCl. Filtrateswere concentrated under reduced pressure subsequentlyprecipitating more KCl which was filtered to obtain filtrate containing desired alkyltrimethylammonium carboxylates5a-e in quantitative yields. Solutions were dried first underreduced pressure and followed by high vacuum. However,due to increased solubility of KCl in the presence of theproducts up to 3% of KCl remains in the final product asdetermined by AgNO3 titration and TG analysis.
10108-87-9, As the paragraph descriping shows that 10108-87-9 is playing an increasingly important role.
Reference£º
Article; ?tanfel, Ur?a; ?ener, Bo?tjan; Be?ter-Roga?, Marija; Ko?mrlj, Janez; Medo?, ?iga; Virant, Miha; Acta Chimica Slovenica; vol. 67; 1; (2020); p. 270 – 275;,
Metal catalyst and ligand design
Ligand Template Strategies for Catalyst Encapsulation – NCBI