With the rapid development and complex challenges of chemical substances, new drug synthesis pathways are usually the most effective.148332-36-9,[2,2′:6′,2”-Terpyridine]-4′-carboxylic acid,as a common compound, the synthetic route is as follows.,148332-36-9
Take the material according to the following specific mass or volume:Htpc (27.7 mg, 0.1 mmol),CrCl3¡¤6H2O (40 mg, 0.15 mmol),DMF (12.9 mmol, 1 mL),CH3CN (1mL),H2O (9mL),HNO3 (21 uL, 7 mol/L).The above materials were placed in a 25 mL reaction kettle.Stir for 0.5 to 1.5 hours,Warming up to 120 ¡ã C,After 3 days of reaction,Naturally cooled to room temperature,Light red crystals were observed,Is the target product,Filter it out of the mother liquor,Water washing,It is naturally dry after finishing.
148332-36-9 [2,2′:6′,2”-Terpyridine]-4′-carboxylic acid 2762749, acatalyst-ligand compound, is more and more widely used in various fields.
Reference£º
Patent; Chongqing Normal University; Chen Xin; Zhang Ruyi; Huang Kunlin; Ding Xumeng; Guo Yuanyuan; (9 pag.)CN108997432; (2018); A;,
Metal catalyst and ligand design
Ligand Template Strategies for Catalyst Encapsulation – NCBI