29176-55-4, 2,9-Dichloro-1,10-phenanthroline is a catalyst-ligand compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
To a 100 mL flask was added 1245 mg (5.0 mmol) of 2,9-dichloro-phenanthroline,2160 mg (20.0 mmol) of N-allylimidazole,1500 mg (10.0 mmol) of sodium iodide (NaI)40 mL of toluene,In the 110 ~ 120 oil bath,The reaction was stirred for 96 hours.The resulting precipitate is filtered,Washed with toluene (2 x 15 mL)Ether wash (2 x 15 mL),With hot water to dissolve,Filtered and added dropwise to an aqueous solution of 3260 mg (20.0 mmol) of ammonium hexafluorophosphate (NH4PF6)The precipitated solid was dried to give the off-white powder as the ligand precursor product S1,Yield: 1026 mg (30%)., 29176-55-4
29176-55-4 2,9-Dichloro-1,10-phenanthroline 355196, acatalyst-ligand compound, is more and more widely used in various.
Reference£º
Patent; Sinopec Corporation; Sinopec Corporation Shanghai Petrochemical Institute; Liu Bo; Jin Zhaosheng; Li Yanan; Lv Jiangang; Sun Lanping; Huang Zujuan; (19 pag.)CN105085553; (2017); B;,
Metal catalyst and ligand design
Ligand Template Strategies for Catalyst Encapsulation – NCBI