Some tips on 4062-60-6

The synthetic route of 4062-60-6 has been constantly updated, and we look forward to future research findings.

4062-60-6,4062-60-6, N1,N2-Di-tert-butylethane-1,2-diamine is a catalyst-ligand compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated

A suspension of 30.1 mg (3-isobutyryl-6-methoxy-lH-indazol-l-yl)acetic acid in 1 mL DCM was treated with 38 muL oxalyl chloride and 10 muL DMF at room temperature for 2.5 hours. The reaction mixture was evaporated to dryness and the residue taken up in 1 mL dry DCM and treated with 8.6 mg N^-di-tert-butylethane-l^-diamine and 15 muL triethylamine over night. Purification of the reaction mixture on RP-etaPLC afforded the title compound following lyophilization. LC-MS: 4.19 min. (m/Z: 711.5, 689.5, 577.4, 633.5).

The synthetic route of 4062-60-6 has been constantly updated, and we look forward to future research findings.

Reference£º
Patent; MERCK & CO., INC.; WO2008/30390; (2008); A2;,
Metal catalyst and ligand design
Ligand Template Strategies for Catalyst Encapsulation – NCBI