Top Picks: new discover of N1,N2-Diphenylethane-1,2-diamine

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Diazomethyl Ketone Derivatives of Pyrimidine Nucleosides

1,5,6,8-Tetradeoxy-8-diazo-beta-D-erythro-7-octulofuranosylthymine (20) and 5,6,8-trideoxy-8-diazo-beta-D-ribo-7-octulofuranosyluracil (31), pyrimidine nucleosides containing the reactive diazomethyl ketone function, were prepared from thymidine and uridine via their 5′-aldehydes 2 and 22 by the Wittig reaction with (carbalkoxymethylene)triphenylphosphoranes followed by modification of the side chains of 3, 4, and 23 and blocking of the acidic NH of the pyrimidine rings.

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Reference£º
Metal catalyst and ligand design,
Ligand Template Strategies for Catalyst Encapsulation – NCBI